Phenix

Low Temperature Chamber for Powder Diffraction

The Phenix stands out as a closed-cycle cryostat exclusively designed for powder diffraction applications. Its compact sample chamber not only provides convenient access but also accommodates a variety of flat-plate sample holders made from different materials. It integrates with a variety of vertical powder diffractometers and is capable of operating in both theta-theta and theta-2 theta modes.

Benefits

  • Temperature Range:  12-290 K
  • Cryogen:  Helium (Closed-Cycle)
  • Fast Cooldown:  20K in 40 mins
  • 12 K in 60 mins
  • Fast Warm-Up:  12 K to room temp in 45 mins
  • Stability:  +/- 0.1 K

Typical Applications

  • Materials science experiments down to 12 K
  • Phase identification, quantitative analysis and determination of structural imperfections
  • Determination of crystal structures and extraction of 3-D micro-structural properties
  • Phase transitions down to 12 K

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Phenix Chamber
Window MaterialKapton
Sample Mounts⌀ 20 mm chromium-plated copper*
K450 Helium Compressor
Weights & Dimensions64 x 61 x 54 cm, 100 kg
Supply Fuse Rating20 A (Starting Current: 65 A)
Cooling Requirements3kW Water Chiller or plumbed supply
Flow rate 5l/min at 18°C

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* Included (2 flat, 2 recessed)

 Water Chiller not provided

Mechanical Cooling

The Phenix incorporates our two-stage Gifford McMahon (GM) cryocooler. Operating in a closed helium circuit, it consumes no helium gas to achieve the desired temperature. Cooling occurs via heat conduction between the sample stage and the cryocooler’s cold stages, with sample temperature measured at the stage itself.

Radiation Shield

Heat leaks within the Phenix are reduced by a radiation shield incorporating 0.005mm mylar windows, and the robust Phenix lid incorporates X-ray transparent windows of 0.25mm carbon fibre.

Sample Plates

A number of 20mm diameter chromium plated copper sample stages are provided with the Phenix system, including flat plate and recessed copper holders. Different materials are also available on request.